n-Heptane for Synthesis

Normal Heptane , Heptyl hydride

Specifications

CERTIFICATE OF ANALYSIS
Name of the Sample : n – Heptane for Synthesis
Batch No. : 33989563
Date of Mfg : July 2022
Date of Exp : July 2025
Register No. : 2021-22
Qty of Sample : 500ml
Date of Analysis : July 2022
S. No Test Parameters, Observed Values, Standard Values
1. Description, Passes, A clear colorless liquid
2. Assay (GC area %), 99.35%, Min.99.0%
3. Wt. per ml at 20°C, 0.683gm, 0.680-0.685g
4. Refractive Index, 1.387, 1.387-1.388 (20°C; 589 nm)

Oil Production by Hexane Solvent Extraction

Solvent extraction consists of a sequence of four operations:
(1) physical removal of oil from the seed in the extractor;
(2) desolventizing-toasting of the de-oiled seeds, often combined with drying and cooling of the meal;
(3) distillation to remove the solvent from the extracted oil;
(4) recovery of the solvent, for reuse in the extractor. The solvent is almost always hexane, which satisfies the technical, economical, and operational needs of all oil millers. Several other solvents have been studied but their disadvantages are such that they cannot compete with hexane, which has many compensatory advantages despite being flammable (Dijkstra and Segers 2007).

The industry generally makes a distinction between two types of extractor: percolation type and immersion type. The percolation process, also known as the continuous extraction process, is based upon the principle of uninterrupted passage of the solvent through the bed of oleaginous material; the oil is thus dissolved in the solvent and carried away. In the immersion process, the entire load of seeds is immersed in solvent. The system is static, so it needs to be stirred to balance the differences in the oil–solvent concentration. Stirring inevitably causes abrasion of the extraction material, so the mixture needs subsequently to be filtered out. This method is used when it is not easy to extract the oil from the matrix. Oil extractors can also be classified on the basis of other different criteria, such as basket or belt operation, rotary or straight, or other shapes, full or partial countercurrent operation, etc.; however, it must be underlined that today the systems available in the market are becoming more and more similar to each other (Fils 2000). The oil-saturated solvent obtained from the extraction process is referred as “miscella.” All commercial extractors are today based on the principle of countercurrent extraction. Fresh solvent encounters previously extracted material, whereas new seeds, flakes, or collet encounter solvent already containing some oil. This method is able to remove a high level of oil using a little solvent quantity (Anderson 2011). Temperature is one of the key variables to keep under control and to optimize the extraction process. The boiling point of hexane is about 69°C near ambient pressure. However, it becomes an azeotrope in the presence of water or steam, with a boiling temperature of 61.6°C. It would be desirable to operate close to the temperature point of this azeotrope; it is the hottest temperature reachable before hexane evaporation, thus it would allow to obtain the lowest viscosity of both solvent and oil and consequently to promote a rapid oil solubilization (Anderson 2011). The length of the extraction process is determined by several factors that affect the contact time between the solvent and the oleaginous material, required for a best extraction yield. Among these factors, the oil concentration, the viscosity of solvent and oil, the shape and size of solid particles and their resulting specific internal structure after pretreatment, are essential to calculate the residence time of the solvent in the extractor. Simulations reported that the greatest amount of oil is extracted during the first minutes, being the oil less accessible to the solvent in the last phase due to equilibrium phenomena (Anderson 2011).

After oil extraction, the meal contains 25%–35% of solvent, which must be evaporated and recovered for reuse (Nagaraj 2009). On the other hand, the de-oiled meal is toasted to reduce anti-nutritional factors such as glucosinolates or trypsin inhibitors, which act as antigrowth factors in monogastric animals if the meal is incorporated into animal feed. Moreover, the meal should be dried to minimize the risk of biological contamination and cooled close to room temperature to remain flowable during storage and transport. The process known as desolventizing, toasting, drying and cooling process (DTDC), invented by Schumacher (1985), combine all these operations in a single piece of equipment (Kemper 2011). The most widely used equipment today is the vertical stack consisting of a number of chambers separated by trays. The meal enters at the top and is conveyed downward while being mixed by agitating sweeps anchored to a central rotating shaft. The heat needed for increasing meal temperature and evaporating the solvent is supplied by steam, which is directly and indirectly introduced into the meal via the trays. When indirectly heated using a steam jacket, hexane will evaporate and the temperature will not rise above the boiling point of hexane. Moreover, in this way, live steam will not condense on the flakes, thus allowing a control of the moisture level during the next steps. The reduced moisture, however, provides less protection against overheating, which may lead to a significant decline of the nutritional value during toasting. Subsequently, the material is heated with live steam, which will condense and raise the temperature above the boiling point of hexane that will be completely vaporized. Additionally, the condensed steam humidifies the meal to a point where a good toasting is possible. In the next chamber, the desolventized meal is cooled and dried by air. Heated air is passed over the material to dry it, at the same time, outside air is blown through the material to cool it. Furthermore, the hot air, while drying, also cools the material and the cold air, while cooling, also dries the material (Kemper 2011).

The miscella leaves the extractor with a 25%–30% oil content, which is separated from the solvent by evaporation of the latter. The miscella evaporator, also referred to as economizer, utilizes the latent heat contained in the vapors leaving the desolventizer to evaporate the solvent till an oil concentration of 65%–75%. The concentrated miscella may then undergo to a second step of solvent evaporation, which utilizes the sensible heat of the condensate steam coming from the DTDC. The residual hexane is then removed by vacuum stripping. The evaporated solvent must be cooled in a condenser and cleaned into a mineral absorption system before being reused in the extractor (Dijkstra and Segers 2007).

Junyuan Petroleum Group donated money to help Heze fight epidemic

The epidemic situation is merciless, but people are sentient and work together to tide over the difficulties. In August, the situation of epidemic prevention and control in Heze City was extremely severe. In order to help Heze City win the sniper battle of epidemic prevention and control, on August 2, Junyuan Petroleum Group, the parent company of Dongying Liangxin Petrochemical Technology Development Limited Company actively supported Heze City and donated 50,000 yuan to the Red Cross Society of Heze City for the prevention and control of COVID-19 epidemic in Caoxian county and Mudan District. It practiced the responsibilities and responsibilities of private enterprises with practical actions, and gathered the positive energy of working together to overcome difficulties.

In recent years, Junyuan Petroleum Group, the parent company of Dongying Liangxin Petrochemical Technology Development Limited Company, has made positive contributions to social welfare undertakings while achieving rapid development. Participated in the educational activities organized by Dongying Civil Affairs Bureau, and donated 100,000 yuan at one time; Participated in the targeted poverty alleviation and Charity Day donation activities in Dingzhuang Town, Guangrao County, and donated 130,000 yuan; In response to the targeted poverty alleviation activities of Guangrao County Charity Federation, donated 200,000 yuan; In the year of COVID-19, the company donated 500000 yuan to Dingzhuang sub district Charity Federation and donated prevention and control materials to surrounding villages and epidemic prevention and control points under the condition that its production and operation were seriously affected.

Next, Junyuan Petroleum Group, Dongying Liangxin Petrochemical Technology Development Limited Company’s parent company, will continue to practice the responsibilities and responsibilities of private enterprises and make positive contributions to social development.

The Junyuan Petroleum Group of Companies participated in the Symposium on project docking between financial leasing companies and small and medium-sized enterprises

On the morning of July 29, Dongying local financial supervision bureau held a symposium on the project docking between financial leasing companies and small and medium-sized enterprises. At the symposium, a number of financial leasing companies in Shandong Province were invited to carry out project face-to-face exchanges and interactions with small and medium-sized enterprises to carry out financing docking. Che Xiaojing, executive deputy general manager of the asset management company, attended the meeting and introduced the company’s projects.

The meeting pointed out that all financial leasing companies should take serving the real economy as the starting point and foothold, put forward reasonable financing plans and suggestions according to the financing needs of enterprises, help enterprises finance, and achieve steady development in the process of promoting local economic development. Small and medium-sized enterprises should further understand and be familiar with the financing method of financial leasing, effectively use financial leasing to alleviate capital problems, take the initiative to strengthen the connection with financial leasing companies, and invite financial leasing companies with promising cooperation to visit the enterprise on the spot to strive for cooperation.

Dongying Liangxin Petrochemical Technology Development Limited Company
Dongying Junyuan Petrochemical Technology Development Limited Company

The emergency management department held a quarterly Video Conference on centralized management of safety risks of hazardous chemicals

On July 29, the emergency management department held a quarterly video promotion meeting on the centralized management of safety risks of hazardous chemicals nationwide to report progress, analyze problems, exchange practices, strengthen measures, promote the implementation of key tasks, effectively prevent and control major safety risks, and create a stable safety environment for the success of the 20th CPC National Congress. Sunguangyu, member of the Party committee and vice minister of the emergency management department, attended the meeting and delivered a speech. Qichunxiao, the general manager of the group, and Qiao Huijie, the deputy general manager and director of safety and environmental protection, attended the video conference at the venue of the agricultural high-tech division in the Yellow River Delta.

However, from the mid-term evaluation results of centralized governance, there are still problems of uneven progress between regions, lagging progress of some special projects and low quality.

The meeting emphasized that we should have a clear understanding of the severe situation faced by the current safe production of hazardous chemicals and strengthen the sense of mission and urgency of doing a good job in centralized management. We should adhere to the problem orientation, anchor the goal of centralized governance, and make every effort to overcome difficulties. We should quickly wake up, be nervous, and take action. If there is a deviation in the direction of work, we should correct it in time. If the progress of work lags behind, we should pay close attention to make-up lessons, and accelerate the completion.

The meeting required that we should adhere to both the symptoms and root causes, accurately grasp the relationship between major risk prevention and control and centralized governance, promote major risk prevention and control and centralized governance as a whole, and prevent “two skins”. We should organically integrate centralized management and annual key work, integrate the requirements of centralized management tasks and measures into the major inspection of production safety and special safety actions, strengthen supervision and inspection and open and secret visits, do a good job in production safety in summer and flood seasons, strictly implement the main responsibility of enterprises, and resolutely prevent and contain major accidents and accidents with great impact.

At the meeting, Beijing, Liaoning, Zhejiang, Ningxia and other four provinces and CNPC made exchange speeches respectively, and the heads of relevant departments and bureaus, institutions and industry associations of the emergency management department and the main heads of relevant central enterprise safety management departments attended the meeting at the main venue; The heads of the emergency management departments at the provincial, municipal and county levels, as well as the relevant chemical parks and the main heads of enterprises attended the meeting at the branch venue.

Dongying Liangxin Petrochemical Technology Development Limited Company

Graduate students from Ocean University of China come to our company for exchange and visit

On the morning of July 22, a group of 5 graduate students majoring in Applied Chemistry from Ocean University of China came to our company for exchange and visit. Sun peisheng, the assistant general manager of the company, Wei fuchang, the director of the production and operation center, and chen huimin, the manager of the general office, attended the exchange.

Chen Huimin extended a warm welcome to the exchange students of Ocean University of China and introduced the company in detail. The graduate students listened carefully to the introduction and watched the company’s promotional videos. Wei fuchang led the exchange students to visit the factory and gave relevant explanations. Sun Peisheng had in-depth exchanges with students in the company’s products, research directions, cooperation fields and other aspects. This activity created opportunities for communication and learning between the company and the school, and laid a good foundation for the next step of school and enterprise cooperation.

Dongying Liangxin Petrochemical Technology Development Limited Company

Dongying Vocational College of Science and Technology visited our Company for Exchange and Investigation

On the morning of July 13, Miao Jin, Dean of the school of Economics and Management of Dongying Vocational College of Science and Technology, and his delegation came to our company for exchange and investigation. Chen Huimin, Manager of the General Office of the company, participated in this exchange activity. Chen Huimin extended a warm welcome to the leaders of the college, and the two sides had an in-depth exchange and Discussion on how to deepen school and enterprise cooperation. Miao Jin expressed the hope to reach long-term practical training friendly cooperation with the company.

Through this exchange activity, the communication and understanding between the company and the school have been strengthened, the friendly relationship between the two sides has been enhanced, and the foundation has been laid for further cooperation.

Dongying Liangxin Petrochemical Technology Development Limited Company, a subsidiary of Junyuan Petroleum Group, has been engaged in the export of butane, pentane, hexane and heptane since 2006. More than 15 years of experience enables you to rest without worrying about goods transportation.

Major customers include PetroChina, Sinopec, Shell, BASF, Saudi Basic Industries Corporation, China Coal, geothermal power plants and other foaming plants.
SGS, CIQ, BV, Rosh, ISO certificates are available.
Production Capacity: 1000,000 tons / year
After Sales Service: Dongying Liangxin Petrochemical Technology Development Limited Company enjoys a good reputation in the alkane industry. You can trust us completely.
Quality Assurance
As a quality-oriented company, we spare no effort to provide customers with the best range of products. In addition, we have hired a team of quality analysts to ensure that our industrial chemicals series meet international standards. Our quality analyst team maintains strict monitoring of the handling of chemicals and ensures that the range of various parameters is checked before sending chemicals to the client. The various parameters of our csindustrial chemical series tests are as follows:
Pure
PH value
Precise composition
For more information: info@junyuanpetroleumgroup.com